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P2704-MRT - MOSH/MOAH in spelt (LC-GC-FID and GCxGC-FID, ring systems)

EPTIS Ringversuch Nr. 1648762 | Letze Änderung 2026-11-11 | URL: https://www.eptis.bam.de/pts1648762 https://www.eptis.bam.de/pts1648762

Name des Anbieters
Name des Anbieters PROOF-ACS GmbH PROOF-ACS GmbH
Ansässig in Germany
Sprache(n) English
Anmerkungen Analysis of MOSH and MOAH by LC-GC-FID is a routine technique nowadays, while the analysis by GCxGC-FID is more advanced and is applied for quantification of MOAH separately for the different ring systems. P2704-MRT offers laboratories the choice to quantify the material - by LC-GC-FID for total MOSH and total MOAH, and/or - by GCxGC-FID for MDAF (mono- and diaromatic fraction) and TPAF (tri- and polyaromatic fraction), and total MOAH according to their needs. A full validation of both analytical methods cross the techniques is possible if both modules are chosen. Attention: Please make sure that you choose the correct technique for your lab and your instrumentation! A spiked sample of milled spelt (flour) and the corresponding unspiked milled spelt are provided as test material and blank material. An LOQ of total MOAH of 0.5 mg/kg is required in accordance with the expected maximum levels. Spiked levels are within the typical ranges of contaminations of the respective matrix. The results related to the spiked materials are evaluated with respect to the comparability criterion (z-score) as well as with respect to the trueness criterion (70 to 120 % of the spiked level, as far as scientifically reasonable). P2704-MRT is offered as a method ring test, which means, - the evaluation is not limited to the pure statistical evaluation. - the participants are asked to provide the chromatograms and plots related to the test materials. - the participants are asked to answer a questionnaire related to relevant aspects of the sample preparation and analysis. The chromatograms as well as the answers related to the questionnaire are summarised in separate parts of the final report. For reasons of fairness, only those participants, which provide details and chromatograms will receive these parts of the report. The data will help to identify shortcomings, built the basis for further discussion and thus help to enhance the quality of the applied method.
Klassifizierung
Produktgruppen Food and drink
Prüfgebiete Analytical chemistry
Technische Einzelheiten
Prüfobjekt Prüfeigenschaft Prüfmethode
Spelt (milled) MOSH C10 - C50 LC-GC-FID
MOAH C10 - C50 LC-GC-FID
GCxGC-FID
MDAF (mono- and diaromatic fraction) GCxGC-FID
TPAF (tri- and polyaromatic fraction) GCxGC-FID
Ringversuchsziele
Zielgruppe des Ringversuchs
Relevante Rechtsvorschriften oder Normen
Weitere Ziele
Teilnehmerzahl 10
Anbieter unabhängig überprüft (akkreditiert, benannt, anerkannt)

Akkreditiert durch DAkkS auf der Grundlage von 17043

Die Durchführung des Ringversuchs ist in Auftrag gegeben durch
Kosten
Teilnahmegebühr 1110 Euro
Regelmässig durchgeführt Nein (Zuletzt 2027)
Wann wird der Ringversuch wieder durchgeführt
Kontaktdaten des Anbieters
Anbieter Kontaktperson
PROOF-ACS GmbH
Gottlieb-Daimler-Str. 1
28237 Bremen
Germany

Telefon: +49 (0)421 388 928 50
Fax:
Web: http://www.proof-acs.de http://www.proof-acs.de
Dr. Birgit Schindler
Telefon: +49 (0)421 388 928 54
Fax:
E-Mail: proof@proof-acs.de proof@proof-acs.de
Haben Sie einen Fehler entdeckt? Bitte wenden Sie sich an den zuständigen EPTIS Koordinator für Germany, Mr Johannes van de Kreeke. Mr Johannes van de Kreeke.
Haben Sie Fragen? Senden Sie uns eine E-Mail: eptis@bam.de.
Anwendungsversion: 1.23-SNAPSHOT.20230502124635-7925ae379a631fc1ececff45d2921c8db38877d5